Hi @Asma ,
Normally, deleting a blocklist entry should take effect immediately. Please confirm that the email address in your block list has been successfully deleted. It is better if you can provide any screenshot.
Manage allows and blocks in the Tenant Allow/Block List | Microsoft Learn
To double confirm, use the Get-TenantAllowBlockListItems cmdlet to view entries in the Tenant Allow/Block List.
Get-TenantAllowBlockListItems -Entry <your email address> -Block
Get-TenantAllowBlockListItems (ExchangePowerShell) | Microsoft Learn
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